XH-300PE High Voltage Ultrasonic Microwave Combination Workstation Introduction: The XH-300PE Magicube high-pressure ultrasonic microwave collaborative combination workstation is a new generation of multifunctional combined microwave chemistry workstation that combines microwave, ultrasonic, and high-pressure functions together. It is the first time at home and abroad to combine microwave ultrasonic collaborative combination technology with microwave high-pressure technology. By utilizing the fast and selective heating of microwaves, the oscillation, dispersion, and cavitation effects of ultrasonic waves, as well as the advantages of increasing solvent boiling point and accelerating molecular motion under high-pressure systems, it realizes the collaborative treatment of microwave and ultrasonic waves under high-pressure systems. This instrument integrates various types of instrument functions into one, and can simultaneously achieve multiple functions such as atmospheric pressure, high pressure, liquid phase, solid phase, microwave, ultrasonic, ultraviolet, single station exploration, multi station parallel amplification, atmosphere protection, etc., with high integration. The combination of ultrasonic high-pressure system and microwave-assisted heating greatly improves the uniformity of nanomaterial synthesis and reduces the probability of nanoparticle aggregation; Simultaneously applied to the extraction of active ingredients from natural products, metal mineral leaching, and other fields, effectively improving the leaching rate. Technical parameters: Instrument model: Magicube XH-300PE microwave system Microwave frequency: 2450MHz; Microwave power: 0~1000W/0~2000W continuously and automatically adjustable; Adopting PID automatic frequency conversion control technology. Ultrasound System Ultrasonic power: 0~1500W continuously adjustable; Working environment: 0~300 ° C; Ultrasonic frequency: 25 ± 1KHz; Ultrasonic titanium alloy probe: one each with a diameter of 8mm and 18mm, suitable for reaction vessels of different volumes; Ultrasonic pulse: The proportion of working time can be adjusted arbitrarily; Ultrasonic transducer: equipped with automatic frequency searching and locking function, capable of maintaining maximum sound power when the properties and viscosity of reactants change; The ultrasonic transducer is enclosed and cannot be exposed or accessed Pull out the upper part to avoid safety hazards such as electric leakage and microwave leakage; Working mode: Constant power mode; Continuous operation for 99 hours, with adjustable ultrasonic pulse time UV light system: (optional) Ultraviolet wavelength: 365nm, power: 250W; Off band ultraviolet stray light: UV365<0.02% Temperature controller Temperature sensor: using Pt1000 high-precision contact temperature sensor; Scope: Temperature control range of atmospheric pressure system; 0~300 ° C; Temperature control range for microwave high-pressure system: 0~260 ° C, temperature control range for microwave ultrasonic high-pressure system: 0~240 ° C; Accuracy: Temperature measurement accuracy: ≤± 0.1 ° C; Temperature control accuracy: ≤± 1 ° C; Display accuracy: 1 ° C; Temperature setting: intelligent temperature control self-learning function, fully automatic intelligent adjustment of insulation power; Various algorithms such as constant temperature mode, rate heating, power heating, etc. Pressure control system Scope: Maximum working pressure of microwave high-pressure system: ≥ 6MPa, maximum working pressure of microwave ultrasonic high-pressure system: ≥ 4MPa, pressure measurement accuracy ± 0.01MPa, detection frequency 150-200 data/second; Pressure sensor range: 0~10MPa; Accuracy: Measurement accuracy: 0.01MPa; Dual temperature/pressure measurement and control system: Real time detection of temperature/pressure changes in the reaction system. When the set temperature/pressure value is reached, the instrument automatically controls the temperature and pressure. When any measured value of temperature or pressure exceeds the standard, the instrument automatically alarms and cuts off power transmission; . Explosion proof design: The tank body is radially vertical to avoid lateral impact. Reactor cavity system Microwave high-capacity resonant cavity: made of austenitic non-magnetic stainless steel material, pressed as a whole; The bottom steel plate integrated structure (can be riveted and welded with different materials) has good corrosion resistance and microwave reflection performance; Chamber door: Industrial grade impact resistant design, high-strength non deformable structure, sealed and sealed, effectively preventing microwave leakage; Open reaction unit: droplet funnel and condenser tube can be installed for reflux reaction; Microwave atmospheric pressure reaction volume: 10-2000ml; Super strong single point magnetic stirring: The stirring speed is infinitely adjustable and suitable for both microwave atmospheric pressure and microwave high-pressure conditions, with real-time display of stirring speed; The speed is 1400rpm, and the stirring rate is infinitely adjustable; High pressure sealed reaction unit Pressure resistant outer tank: made of fully imported high-strength composite PEEK material, with a fully enclosed structure and good sealing performance, high pressure resistance Inner tank: made of molded polytetrafluoroethylene material, with good density and good safety performance without micropores; Microwave high-pressure reactor volume: 100ml, pressure resistance of 0-6MPa; Microwave medium pressure reactor volume: 250ml, pressure resistance 0~4MPa; Microwave low-pressure reactor capacity: 500ml, pressure resistance 0~2MPa; Instrument control system Setting reaction parameters: The instrument can set 20 reaction stages in steps, and each working stage can be set arbitrarily. It can also be set in stages, including ultrasonic power and duty cycle, microwave power, temperature, pressure, time and other parameters. Different working modes can be selected, and multiple reaction data sets can be stored without limitation; . Real time curve: Real time display of ultrasonic power and duty cycle, microwave power, temperature, pressure, time, pressure value and curve in the reaction system; Data organization: Export data/record images/videos through USB interface, play them back on the computer for data analysis; Advanced intelligent temperature control self-learning function, fully automatic intelligent adjustment of insulation power; Remote control: stop reaction from a distance in emergency situations;
Introduction: The XH-300PE Magicube high-pressure ultrasonic microwave collaborative combination workstation is a new generation of multifunctional combined microwave chemistry workstation that combines microwave, ultrasonic, and high-pressure functions together. It is the first time at home and abroad to combine microwave ultrasonic collaborative combination technology with microwave high-pressure technology. By utilizing the fast and selective heating of microwaves, the oscillation, dispersion, and cavitation effects of ultrasonic waves, as well as the advantages of increasing solvent boiling point and accelerating molecular motion under high-pressure systems, it realizes the collaborative treatment of microwave and ultrasonic waves under high-pressure systems. This instrument integrates various types of instrument functions into one, and can simultaneously achieve multiple functions such as atmospheric pressure, high pressure, liquid phase, solid phase, microwave, ultrasonic, ultraviolet, single station exploration, multi station parallel amplification, atmosphere protection, etc., with high integration. The combination of ultrasonic high-pressure system and microwave-assisted heating greatly improves the uniformity of nanomaterial synthesis and reduces the probability of nanoparticle aggregation; Simultaneously applied to the extraction of active ingredients from natural products, metal mineral leaching, and other fields, effectively improving the leaching rate.
